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Bruker Daltonics today has released a robust, fast and highly sensitive
high-capacity ion trap HCT™ solution for the detection and
quantification of melamine and cyanuric acid (CA) by food safety
laboratories.
Since September 2008, thousands of infants and young children in China
have been hospitalized to treat the symptoms caused by the ingestion of
melamine and CA contaminated infant formula and related dairy products.
Previously in 2007, pet food, animal feed wheat gluten and other
protein-based foods were found to contain residues of melamine and CA.
A five minute, accurate LC-MS/MS analysis method has been developed by
Bruker Daltonics’ food safety development laboratory in Australia. This
robust, easy-to-use and cost-effective method for the extraction,
detection and quantification of melamine and CA uses the speed,
sensitivity and excellent quantitative capabilities of the high-capacity
ion-trap mass spectrometer HCTultraTM,
hyphenated with a Dionex UltiMateTM 3000 LC system and AcclaimTM
Mixed-Mode WAX-1 column. The method is capable of detecting melamine in
various matrixes well below the concentrations required by various food
safety and other regulatory authorities around the world, such as the
limits set by the U.S. Food and Drug Administration (FDA) of 1 ppm for
melamine and cyanuric acid in infant formula, and 2.5 ppm for other
foods.
Dr. Matthias Pelzing, Asia-Pacific Applications Manager for Bruker
Daltonics, explained: “We recommend LC-MS/MS methods due to their
straight-forward sample preparation, compared to GC-MS methods which
often require sample derivatisation. With our new routine analysis
method we have demonstrated that melamine can be detected down to trace
levels of 0.05 ppb, and that it is possible to quantify melamine at
concentrations relevant to various international food authorities in 5
minutes.”
Mr. Clive Seymour, Executive Vice President of Bruker Daltonics,
commented: “Due to its robustness, ease of use, small footprint and
lower cost, our HCT ion trap-based solution offers significant practical
and operational advantages over traditional triple-quad MRM approaches.
In addition, the superior full scan sensitivity of our unique HCT ion
trap technology offers not only outstanding detection limits for
melamine and CA, but also the option of full-scan identification of
other unknown, new or modified food contaminants with superior
sensitivity.”
The new Bruker Application Note # LCMS-49 on melamine and CA analysis is
available in English, Chinese, Korean, Thai and Japanese, and can be
down-loaded at www.bdal.com.
UltiMate and Acclaim are registered trademarks of Dionex Corporation.
For more information about Bruker Daltonics and Bruker Corporation
(NASDAQ: BRKR), please visit www.bdal.com
and www.bruker.com.